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Standard Test Method for Measuring Reaction Rates by Analysis of Molybdenum-99 Radioactivity From Fission Dosimeters (Withdrawn 2002)
通过分析裂变剂量计的钼-99放射性测量反应速率的标准试验方法(2002年撤销)
发布日期:
1996-01-01
废止日期:
2002-06-10
1.1本试验方法包括通过测定裂变产物的量来测量反应速率
99
非阈值反应产生的钼
241
Am(n,f),
235
U(n,f),和
239
Pu(n,f)和阈值反应
238
U(n,f),
237
Np(n,f),和
232
Th(n,f)。
1.2这些反应产生许多裂变产物,其中包括
99
钼的半衰期为65.94小时。由于在完成伽马射线能谱测定时未分辨或干扰伽马射线,其他裂变产物的竞争活动需要采用化学分离来分离
99
瞬间。
99
钼发射几种能量的伽马射线,很容易被伽马射线探测和识别-
射线光谱仪。
1.3使用合适的技术,可以在10范围内测量中子注量率
到大约10
14
n[点]厘米
[点]s
.
1.4用裂变剂量计测量时间积分反应速率
99
Mo分析受到
钼的辐照时间可达300小时左右。
1.5以国际单位制表示的数值应视为标准。
1.6本标准无意解决与其使用相关的所有安全问题(如有)。本标准的用户有责任在使用前制定适当的安全和健康实践,并确定监管限制的适用性。
1.1 This test method covers the measurement of reaction rates by determining the amount of the fission product
99
Mo produced by the non-threshold reactions
241
Am(n,f),
235
U(n,f), and
239
Pu(n,f) and by the threshold reactions
238
U(n,f),
237
Np(n,f), and
232
Th(n,f).
1.2 These reactions produce many fission products, among which is
99
Mo, having a half-life of 65.94 h. Because of unresolved or interfering gamma rays when gamma-ray spectrometry is accomplished, the competing activity from other fission products requires that a chemical separation be employed to isolate the
99
Mo.
99
Mo emits gamma rays of several energies, which are easily detected and identified by a gamma-ray spectrometer.
1.3 With suitable techniques, neutron fluence rates can be measured in the range 10
to approximately 10
14
n[dot]cm
[dot]s
.
1.4 The measurement of time-integrated reaction rates with fission dosimeters by
99
Mo analysis is limited by the half-life of
Mo to irradiation times up to about 300 h.
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.